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  1. 原著論文

Phase stability of fine precipitates and its effect on nano-hardness during isothermal annealing of ITER-grade CuCrZr

https://repo.qst.go.jp/records/2003028
https://repo.qst.go.jp/records/2003028
2beed0ef-757b-48f5-a5ec-643937dd5f43
アイテムタイプ 学術雑誌論文 / Journal Article(1)
公開日 2026-03-25
タイトル
タイトル Phase stability of fine precipitates and its effect on nano-hardness during isothermal annealing of ITER-grade CuCrZr
言語 en
言語
言語 eng
資源タイプ
資源タイプ識別子 http://purl.org/coar/resource_type/c_6501
資源タイプ journal article
著者 Kano Sho

× Kano Sho

Kano Sho

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Hamaguchi Dai

× Hamaguchi Dai

Hamaguchi Dai

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Nozawa Takashi

× Nozawa Takashi

Nozawa Takashi

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抄録
内容記述タイプ Abstract
内容記述 The CuCrZr alloy is a promising candidate for cooling pipes in DEMO fusion reactors, and its secondary phases play a critical role in irradiation integrity and creep properties. This study investigated the stability of fine precipitates and their impact on nano-hardness during isothermal annealing of ITER-grade CuCrZr. Nano-indentation results showed a parabolic decrease in hardness as the annealing temperature increased. The observed softening behavior was governed by two distinct thermally activated processes separated at approximately 673 K. TEM/STEM observations of the as-received specimen confirmed the presence of fine precipitates dispersed uniformly within the intragranular regions. These precipitates were ∼4 nm in size, had a number density of ∼1 × 1023 m⁻³, and exhibited Ashby-Brown, moiré, and loop contrasts. STEM-EDS analysis revealed that these were Cr-rich precipitates and that coarse precipitates, Cr- and/or Zr-rich, were also present. However, the contribution of the coarse precipitates to strengthening was likely negligible due to their low number density. The parameter of Orowan-type dispersion strengthening associated with the fine Cr-rich precipitates () showed a consistent trend with hardness softening. This suggests that the hardening coefficient attributable to these precipitates is ∼60 Pa/m. Maximum softening occurred at 300–400 MPa in the 873 K specimen, with a precipitate size of ∼10 nm and a number density of ∼2 × 10²² m⁻³.
書誌情報 Fusion Engineering and Design

巻 227, 号 115732, 発行日 2026-03
DOI
識別子タイプ DOI
関連識別子 10.1016/j.fusengdes.2026.115732
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