@article{oai:repo.qst.go.jp:00048958, author = {Ni, Youyi and Zheng, Jian and Guo, Qiuju and Wang, Hai and Tagami, Keiko and Uchida, Shigeo and 倪 有意 and 鄭 建 and 王 海 and 田上 恵子 and 内田 滋夫}, issue = {3}, journal = {Journal of Radioanalytical and Nuclear Chemistry}, month = {Jan}, note = {In this study, we developed a method to evaluate the potentially bioavailable fraction of Pu in agricultural soils by determining their water soluble and exchangeable fractions with ion-exchange chromatography and sector field ICP-MS measurement. Three commonly used pretreatment methods were compared to process the extracted solutions. Results showed that these three methods were applicable to obtain consistent Pu concentration results; however, considering the experimental performances and recoveries, we recommended that dealing with the extracted solutions with wet-ashing followed by Fe(OH)3 co-precipitation was the best pretreatment method, with which high Pu recoveries for the whole analytical procedure for water soluble fraction (69.8%) and exchangeable fraction (70.6%) were realized.}, pages = {643--651}, title = {Comparisons of soil pretreatment methods for SF-ICP-MS determination of ultra-trace level Pu in water soluble and exchangeable fractions}, volume = {315}, year = {2018} }