{"created":"2023-05-15T14:35:41.420976+00:00","id":45904,"links":{},"metadata":{"_buckets":{"deposit":"2b44dd84-b1f5-403f-995c-dbbeea788592"},"_deposit":{"created_by":1,"id":"45904","owners":[1],"pid":{"revision_id":0,"type":"depid","value":"45904"},"status":"published"},"_oai":{"id":"oai:repo.qst.go.jp:00045904","sets":["1"]},"author_link":["456642","456638","456639","456636","456637","456640","456641"],"item_8_biblio_info_7":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2010-06","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"22","bibliographicPageEnd":"2993","bibliographicPageStart":"2990","bibliographicVolumeNumber":"51","bibliographic_titles":[{"bibliographic_title":"Tetrahedron Letters"}]}]},"item_8_description_5":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"In the present Letter, a fast, automated, and reproducible method for the synthesis of S-[13N]nitrosothiols is reported. The labeling strategy is based on trapping  in an anion exchange resin. The reaction with thiols in acidic media led to the formation of the desired nitrosothiols in short reaction times (60 s) with excellent radiochemical conversions (from 48.7% to 74.5%). Final radiotracers were purified by HPLC. Good radiochemical yields (from 33.8% to 60.6%, decay corrected) and radiochemical purities (>99%) were obtained in all cases. Stability of the labeled compounds was checked.","subitem_description_type":"Abstract"}]},"item_8_source_id_9":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"0040-4039","subitem_source_identifier_type":"ISSN"}]},"item_access_right":{"attribute_name":"アクセス権","attribute_value_mlt":[{"subitem_access_right":"metadata only access","subitem_access_right_uri":"http://purl.org/coar/access_right/c_14cb"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"Gomez, Vanessa"}],"nameIdentifiers":[{"nameIdentifier":"456636","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Kato, Koichi"}],"nameIdentifiers":[{"nameIdentifier":"456637","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Llop, Jordi"}],"nameIdentifiers":[{"nameIdentifier":"456638","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"et.al"}],"nameIdentifiers":[{"nameIdentifier":"456639","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Ｇｏｍｅｚ Ｖａｎｅｓｓａ","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"456640","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"加藤 孝一","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"456641","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Ｌｌｏｐ Ｊｏｒｄｉ","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"456642","nameIdentifierScheme":"WEKO"}]}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"eng"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"Fully automated synthesis of 13N-labeled nitrosothiols","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"Fully automated synthesis of 13N-labeled nitrosothiols"}]},"item_type_id":"8","owner":"1","path":["1"],"pubdate":{"attribute_name":"公開日","attribute_value":"2010-10-18"},"publish_date":"2010-10-18","publish_status":"0","recid":"45904","relation_version_is_last":true,"title":["Fully automated synthesis of 13N-labeled nitrosothiols"],"weko_creator_id":"1","weko_shared_id":-1},"updated":"2023-05-15T23:58:12.664974+00:00"}