量研学術機関リポジトリ「QST-Repository」は、国立研究開発法人 量子科学技術研究開発機構に所属する職員等が生み出した学術成果（学会誌発表論文、学会発表、研究開発報告書、特許等）を集積しインターネット上で広く公開するサービスです。 Welcome to QST-Repository where we accumulates and discloses the academic research results(Journal Publications, Conference presentation, Research and Development Report, Patent, etc.) of the members of National Institutes for Quantum Science and Technology.
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Ion implantation technique was employed to introduce iron nanoparticles (Fe NPs) into a carbon precursor polymer with the aim for formation of graphitic nanostructure through catalytic graphitization by the introduced Fe NPs. A phenolic resin was implanted by 100 keV Fe+ ions with ion fluence of 1E14-1E16 ions/cm^2 at ambient temperature under vacuum, and subsequently heat-treated at 800°C in nitrogen gas atmosphere. It was found that the particle size of Fe NPs could be controlled in the range of 5-30 nm by the Fe+ ion fluence. Additionally, it was found that nano-sized turbostratic graphite structure with mean interlayer distance of 0.3531 nm, which is consisted of shell-like carbon layers and intricately distorted carbon layers, was formed around the Fe NPs. The ion implantation technique is one of the advantageous ways to introduce size-controlled fine metal NPs which are effective for the formation of graphitic nanostructure from a carbon precursor polymer.
Formation of Fe Nanoparticles by Ion Implantation Technique for Catalytic Graphitization of a Phenolic Resin
